The Amazing Spider-Man #202-203
In "One for Those Long Gone!", J. Jonah Jameson’s desperate bid to catch Spider-Man backfires spectacularly when he funds Dr. Stillwell’s experiment to transform Mac Gargan into the Scorpion—only for the formula to unleash a far more dangerous foe than anticipated. Written by Stan Lee and brought to life with sharp, eerie precision by Steve Ditko, this gripping two-part story sees the Scorpion’s rampage push Spider-Man to his limits, all under the stark, dynamic cover by Keith Pollard and Joe Rubinstein.
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J. Jonah Jameson pays Dr. Stillwell to turn Mac Gargan into the Scorpion to try to capture Spider-Man. Stillwell's formula makes Gargan become more evil than he originally was and the Scorpion goes on a rampage and is finally stopped by Spider-Man.
Plot details indexed by the Grand Comics Database (CC BY-SA).